In collaboration with Scientific Association of Iranian Medicinal Plants

Document Type : Research Paper

Authors

Academic members of Research Institute of Forests and Rangelands, Tehran, Iran

Abstract

 In this research, essential oils were extracted by hydro-distillation method but with different apparatus of distillation from Rosa damascena Mill. The oil obtained at different yields for example for Clevenger (0.008%), Miquel (0.014%), A.O.A.C. (0.012%) and two plans designed in Research Institute of Forests and Rangelands by authors which were named plan-1 (0.015%) and plan-2 (0.023%). Samples were analyzed by GC and GC/MS. The main constituents of the oil by Clevenger were geraniol (26.7%), n-nonadecane (21.3%),  citronellol (12.5%) and n-henicosane (12.0%); by Miquel were geraniol (32.9%), citronellol (19.0%), n-nonadecane (10.6%); by A.O.A.C.  were n-nonadecane (28.5%), geraniol (22.6%), n-henicosane (10.6%) and citronellol (10.2%) in plan -1 were n-nonadecane (21.3%), geraniol( 21.8%), citronellol (12%) and in plan-2 were n-nonadecane (21.8%), geraniol (19.1%) and citronellol (15%),  respectively. By comparison of the results from different apparatus of hydro-distillation, it can be concluded that the best plan for obtaining essential oil from Rosa damascena Mill., were plan-2 and Miquel. 

Keywords

- British Pharmacopoeia, 1988. Vol 2, pp A137-A138, HMSO. London.
- Miquel, J.D., Richard, H.M. and Sandret, F.G., 1976. Volatile constituents of Moroccan Thyme oil. Journal of Agric. Food Chem., 24(4): 833-835.
- Association of Official Analytical Chemists, 1990. Official Methods of Analysis, 15th Edition, Edited by Kenneth Helrich, Volatile oil, page 1001.
- Adams, R.P., 1989. Identification of essential oils by ion trap mass spectroscopy. Academic Press: New York.
- Shibamoto, T., 1987. Retention indices in Essential oil analysis. In: Capillary Gas Chromatography in Essential oils analysis. Edits., P.Sandra and C.Bicchi, p. 259- 274,  Dr. Alferd Huethig Verlag, New York. 
- Davies, N. W., 1990. Gas chromatographic retention index of monoterpenes and sesquiterpenes on methyl silicon and carbowax 20M phases., Journal of Chromatogr., 503: 1-24.
- Rao, B. R. R., Sastry, K. P., Saleem, S. M., Rao, E. V. S. P., syamasundra, K.V. and   Ramesh, S., 2000. Volatile flower oils of three genotypes of rose-scented geranium (Pelargonium sp.), Flavour and Fragrance Journal, 15: 105-107.
- Babu, K. G. D., Singh, B., Joshi, V. P. and Singh, V., 2002. Essential oil composition of Damask rose (Rosa damascena Mill.) distilled under different pressures and temperatures, Flavour and Fragrance Journal, 17: 136-140.
- Reverchon, E., Porta, G. D. and Gorgoglione, D., 1997. Supercritical CO2 extraction of volatile oil from Rose concrete, Flavour and Fragrance Journal, 12: 37-41.
- Karawya, M. S., Hashim, F. M., Hifnawy, M. S., 1974. Oils of jasmine, rose and cassie of egyptian origin, Bull. Fac. Pharm. Univ. Cairo, 13: 183-192.
- Kovats, E., 1987. Composition of essential oil. Part 7. Bulgarian oil of rose (Rosa  damascena Mill.),  Journal of Chromatogr., 406: 185-222.
- Lawrence, B. M., 1991. Progress in essential oils, Perfum. Flavor., 16(3): 43-77.
- Lawrence, B. M., 1997. Progress in essential oils, Perfumer Flavorist., 22 (3): 57-66.
- Guenther, E., 1972. The production of essential oils. In the Essential Oils, vol. 1, Robert E Krieger: Malabar, FL., 87-226.
- Boelens, M. H., 1997. Differences in chemical and sensory properties of orange flower and rose oils obtained from hydrodistillation and from supercritical CO2 extraction. Perfum. Flavor., 22(3): 31-35.